Enabling in-situ XRF measurements

ASSIGNMENT

Enabling in-situ XRF measurements
Contact: Dr. Robbert van de Kruijs (r.w.e.vandekruijs@utwente.nl)

Challenge

  • X-ray fluorescence-based measurements hold structural and chemical information about thin-film samples
  • Possibility to measure during a chemical reaction (operando) or under the reaction conditions (in-situ) often reveals crucial information regarding the prosed inaccessible otherwise.
  • X-ray fluorescence detector is a sensitive tool that can be damaged by harsh environment like pressure or high-temperature.

Application

  • In-situ and operando measurements during chemical reaction, e.g. heterogeneous catalysis   

Task

  • Analyze the potential damage of XRF detecotr
  • Design the possible solutions for protection of XRF detecotr (e.g. cooling, protective window, etc.)


Sensitive XRF detector - Design-focused , applied